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Degradation of organic pollutants including pesticides and herbicides by boron-doped diamond (BDD) was examined. The hydroxyl radical (•OH) was found as a major reactive species in the treatment of pesticides and herbicides with BDD. Next, the effect of various treatments such as dose, temperature and pH on the degradation of pesticides was investigated. Furthermore, the roles of •OH and •NO(2) in the degradation of the pesticides and herbicides were examined by using various scavengers. •OH was found to be the major reactive species in the treatment of all the pesticides and herbicides with BDD